Please use this identifier to cite or link to this item: http://ena.lp.edu.ua:8080/handle/ntb/55797
Title: MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones
Other Titles: Al2O3 Нанесений на MgO: новий, ефективний і відновлювальний каталізатор синтезу хальконів
Authors: Katkar, Santosh Shriram
Kategaonkar, Amol Haridas
Vidhate, Kaluram N.
Affiliation: Science and Commerce College
Milind college of science
Bibliographic description (Ukraine): Katkar S. S. MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones / Santosh Shriram Katkar, Amol Haridas Kategaonkar, Kaluram N. Vidhate // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 169–176.
Bibliographic description (International): Katkar S. S. MgO Supported Al2O3 Oxide: A New, Efficient, and Reusable Catalyst for Synthesis of Chalcones / Santosh Shriram Katkar, Amol Haridas Kategaonkar, Kaluram N. Vidhate // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 169–176.
Is part of: Chemistry & Chemical Technology, 2 (14), 2020
Issue: 2
Volume: 14
Issue Date: 24-Jan-2020
Publisher: Видавництво Львівської політехніки
Lviv Politechnic Publishing House
Place of the edition/event: Львів
Lviv
DOI: doi.org/10.23939/chcht14.02.169
Keywords: оксид Mg-Al
екологічний каталіз
відновлюваність
багатокомпонентна реакція
Mg-Al oxide
environmental catalysis
recyclability
multicomponent reaction
Number of pages: 8
Page range: 169-176
Start page: 169
End page: 176
Abstract: Методом ко-осадження вивчено ряд змішаних оксидів металів Mg-Al, фізико-хімічні властивості яких визначені за допомогою методів РСА, РЕМ, ЕРС, ТЕМ, БЕТ та СО2-ТДС. Розроблено ефективний та простий метод синтезу халконів з використанням різних альдегідів та ацетофенону за допомогою оксиду Mg-Al за умов рефлюксу в етанолі, що забезпечує відмінну продуктивність. Доведено відновлюваність каталізатора, а також здатність MgO до диспергування та підвищення основності, розміру пор і каталітичної активності.
We have studied a series of mixed metal oxides of Mg-Al by a simple co-precipitation technique. Various characterization techniques, including XRD, SEM, EDS, TEM, BET and CO2-TPD were carried out to investigate their physicochemical properties. An efficient and facile protocol has been documented for the synthesis of chalcones using different aldehydes and acetophenone using Mg-Al oxide under reflux conditions in ethanol affording good to excellent yields. Recyclability of a catalyst is a significant feature of this protocol. Moreover, it was proposed that MgO can disperse and increase the basicity, pore size and catalytic activity.
URI: http://ena.lp.edu.ua:8080/handle/ntb/55797
Copyright owner: © Національний університет “Львівська політехніка”, 2020
© Katkar S., Kategaonkar A., Vidhate K., 2020
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[55] Rathod S., Gadekar L., Katkar S. et al., Bull. Catal. Soc. India, 2009, 8, 16.
[56] Shaikh U., Katkar S., Vidhate K. et al.:J. Ind. Chem. Soc., 2012, 88, 1465.
[57] Lande M., Navgire M., Rathod S. et al.:J. Ind. Eng. Chem., 2012, 18, 277. https://doi.org/10.1016/j.jiec.2011.11.048
[58] Vidhate K., Katkar S., Arbad B., Lande M., Adv. App. Sci. Res., 2012, 3, 713.
[59] Katkar S., Kategaonkar A.:J. Chem. Chem. Sci., 2015, 5, 591.
[60] Katkar S., Kategaonkar A., OCAIJ, 2015, 11, 415.
[61] Raghav N., Malik P., Adv.Appl. Sci. Res., 2011, 2, 410
Content type: Article
Appears in Collections:Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 2



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